Post #51 made 14 years ago
So now I've got the crazy idea of trying to squeeze a partigyle out of the spent grains. I've got some extra hops floating around and about a pound of DME I could throw in if needed. I know there's probably not much left in the grains, but I figure even if I could get a small batch out of them it would be better than just trowing the out. I've got a pretty small 2 gallon bucket and a slightly larger 4.25 gallon bucket that I could easily fit with an air lock to ferment in. Any idea what I could expect to get out of my grains? How much water should I go for with the second dunk sparge? I'm also not really sure how to go about planning the hop additions for it. I don't mind winging it though either. Just thought I'd ask.

Post #52 made 14 years ago
Good Day, I would take a gravity reading fro the grain drippings, If it is more than 1.025 You can make a session beer, or what is a "Sunday" 3.25% (small) beer. It was the fashion after "prohibition" was over.
Honest Officer, I swear to Drunk, I am Not God.
    • SVA Brewer With Over 100 Brews From United States of America

Post #53 made 14 years ago
Why not do a big sparge to get a second runnings, then pour those runnings back into the pot and use them as strike liqour for another two or three kilos of grain, and get a standard strength brew out of them? However don't sparge too far to avoid tannin extraction. :peace:

Post #54 made 14 years ago
Well, I brewed this over the weekend and although a lot of fun, it did not quite go as planned. I had a feeling that all of my planning would only get me so far… In the end I had to improvise.

I am however happy to say that I did hit my target OG. I had planned on 1.100 and I'm pretty sure I actually got 1.101. I was also pretty pretty darn close on my final volume. although with out my notes in front of me I can't remember exactly how close.

So, for the problems, they all started when I went to put my grain in and almost overflowed the pot. I had planned with Stux's calculator to have an extra 2L of head space in my pot as a buffer, and believe me, I'm glad I did. I ended up needing all of it. The pot was so full, and the mash was so thick, I could barely stir it. At one point I think the mash was actually above the rim of the pot making putting the lid on almost impossible without spilling. A flaw in my pot design that I had never noticed before is that the lid is actually recessed into the pot by about an inch. I didn't have room for it to set on securely. When I did try put the lid on it actually caused quite a bit of overflow an a pretty big mess on the floor.

I also lost a little more heat than I expected when I added the grains. I ended up having to unwrap my pot and put it back on the heat. A pretty cool thing happened that I never noticed before though. At exactly the same time when i reached my target mast temp 155ºF the grain loosened up and became much easier to stir. It was like magic. I put the lid back on. wrapped it back up and my mash held it's temp for the next hour.

Pulling the grains was also a lot more difficult due to the wait of the grains and the suction effect around the edges of the pot, but in the end, we got it done. We then placed it in the second pot which did not have the full volume of water ready. We learned something the first time so we pulled a few liters off before putting the grain in and then topped it back off with water until full. The second hour long mash/dunk sparge didn't hold temp quite as well as the first but we were still within a couple degrees in the end.

We pulled 7.5L off the first running and boiled them down for almost 2 hours and never got them down to a thick syrup which was fine because I didn't really want to loose more volume than I had to. It was already looking like we were going to be short. And in fact we actually would have been short if I had done the two hour boil as planned. In the end though we decided that anything over an hour was good that we would stop once we hit our target gravity. I think we ended up around 1.5 hours.

The last problem came when I went to use my immersion chiller and discovered that the hose that I usually hook up to the faucet in the back yard was frozen solid with Ice. I had no way to run water through it. I guess I shouldn't have left it outside. So we ended up just filling a tub with cold water and soaking the pot in it for a good 45 min. or so. I figured it wasn't that big of a deal though since we didn't have any flavor or aroma hops to worry about. The only thing that sucked was it put us to about 1:00 a.m. when we were finishing up.

Oh, and I did get about a 3 gallon partigyl with a 1.03 OG out of the grains too. We'll see how that one turn out too.

Post #55 made 14 years ago
Very cool :)

I always suggest reserving a few L when you're doughing in, and then topping back up. I think with your extreme L:G ratio the error in the volume calcs is becoming significant

You experienced a bunch of issues which affected some of my first brews :)

Near overflowing mash, not realizing the lid uses space, being unable to pull the bag, being up waaaay past midnight!

I hope you took plenty of volume/gravity notes, and if so, I would appreciate seeing them, and a copy of your ce calc spreadsheet

Hope the beer comes out fantastic!

Would you say this is a win for the ce calc :)
Fermenting: -
Cubed: -
Stirplate: -
On Tap: NS Summer Ale III (WY1272), Landlord III (WY1469), Fighter's 70/- II (WY1272), Roast Porter (WY1028), Cider, Soda
Next: Munich Helles III

5/7/12

Post #56 made 14 years ago
My actual grain bill ended up being a little less than I should have had. It was about 8.532 kg. where the calc. called for 8.573 kg. ;)

Here are the brands:
17.5 lb. Muntons Maris Otter
.25 lb. Muntons Crystal 150L
.25 lb. Briess Carapils Malt
.25 lb. Briess Roasted Barley
.25 lb. Briess Crystal 120L
.25 lb. Dingemans Special B
.06 lb. Thomas Fawcett Peated Malt

I would say the biggest differences I noticed were in the pot volume. It took up the full 28.3 L (7.5 gal.) of my pot where it should have only taken up 26 L. Also My first run off should have been 13.17 L but my actual was 12.5 L. And I had to really squeeze to get that. But other than that I was pretty happy.

According to the Brew Day results section, I achieved an into fermenter efficiency of 77.6% where your calculator predicted 77.85%. Pretty damn close I'd say. :champ:

Attached is my spread sheet. Let me know if I left out any other details that you would like to know.
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Post #57 made 14 years ago
I think those are pretty spectacular results :)

Adjusting the grain bill to 8.532KG, you actually got 78% Into Fermenter Efficiency for a 1.100 OG beer using BIAB!!!


(I just changed the grainbill field B110 on the details tab to match reality)

And if you had added the 200ml the calculator suggested to dilute then you would have 19.95L of 1.100 wort which is pretty spectacularly spot on ;), with an extra 40g of grain you would've hit 20L or in fact, slightly exceeded it, due to better than predicted efficiency everywhere else than in the conversion.

Absorption turned out to be 1.38L/KG instead of 1.3L/KG. This is probably a very accurate figure, since the grainbill was such a high percentage of the mash. My figures show an absorption value between 1.2-1.4L. 1.38 is quite possibly exactly to be expected. I also think that finer grinds result in less absorption. You might want to consider updating the absorption figure to 1.38L/KG for you next brew. Or not :), by underestimating you normally end up with a more concentrated beer which can be diluted (ie 200ml at the end), where as with the overestimating you end up with a dilute beer... which means a longer boil if you want to rectify it.

8.5KG x 0.08L is the difference, ie 680ml. BUT, that's only 80ml per kilogram of grain.

on the adjusted grain bill you got 96% conversion efficiency. Not too bad for such an extreme grain bill :), and you proved that you can get 1.102 out of a mash with BIAB :)

Now, perhaps the 96% was a bit short than the 99% you were aiming for... but more likely its just a measurement error, or it could be the grains not quite being the same as the specs, or even the milling... it could just be the thick L:G (2.35 L/KG)

I've been using 0.5mm gap on my MM2 mill

anyway, I would estimate that anything >95% is good

1.105 would've been 99% conversion... but that's pretty damn close... and the sparge would've picked up the difference. Quite possible more conversion happened during your second mash.

BTW, with the reduced grainbill, you got 78.0% Into Fermenter which is *exactly* what the calculator has predicted based on the updated grainbill!!!

The mash volume calculation is not actually based on my research, so I'm not *that* disappointed it was off ;)

I found the original factor from the greenbay rackers website... http://rackers.org/calcs.shtml/, Can I Mash It? calculator, 0.67, then added 5% to make it 0.7 for a 5% safety margin. Quite possible it should be higher... I suspect the error is magnified by your thick mash. Anyway, when mashing at the limit, best to hold some water back. Alternatively, I should increase the factor :)


Another thought, did you end up spilling any mash water when you added your lid? That would've lost a few points there

And did you perhaps measure your total mash volume? Might be able to work out a better grain wet displacement figure


I think the big takeaway is that your results were well within the margins of error on your equipment and measuring devices... which means that the CE calc's theory held up in practise on its biggest test yet :)

1) 1.100SG is possible in a BIAB mash.
2) The calculators sparging estimates appear to have been correct
3) the Into/End of boil sparge additions appear to have been calculated correctly...

its all good

Thankyou for you testing this as well, and I really expect the beer will be fantastic :)

I think there is an issue in the chart... as it is getting confused by your -2% Kettle Loss... which I assume is due to measurement inaccuracies somewhere...

Volume measures are probably +-5% and SG +-1%

Amazing results ;)
Fermenting: -
Cubed: -
Stirplate: -
On Tap: NS Summer Ale III (WY1272), Landlord III (WY1469), Fighter's 70/- II (WY1272), Roast Porter (WY1028), Cider, Soda
Next: Munich Helles III

5/7/12

Post #58 made 14 years ago
Just checked, your Into Fermenter efficiency was actually 78.0228%. The calculator predicted 78.0134%

So, rounded to 1 decimal place you actually nailed it :)

Or slightly exceeded it at 2 decimal places ;)

I don't think you can really take an efficiency reading past 1 decimal place anyway.

...

Another way of looking at it...

the calculator was expecting 5.2106KG of extract in the fermenter... (10th of gram accuracy is rubbish ;))

you got 5.2112KG

so 0.6g more than predicted.

50th of an ounce.

That is ridiculously the same. So much so, that the error from the volume and hydro readings are far more significant ;)
Fermenting: -
Cubed: -
Stirplate: -
On Tap: NS Summer Ale III (WY1272), Landlord III (WY1469), Fighter's 70/- II (WY1272), Roast Porter (WY1028), Cider, Soda
Next: Munich Helles III

5/7/12

Post #59 made 14 years ago
stux wrote: I also think that finer grinds result in less absorption. You might want to consider updating the absorption figure to 1.38L/KG for you next brew.
I milled the grain at the LHBS and don't have control over the gap. I did run it through twice though.
Last edited by de5m0mike on 14 Dec 2011, 10:24, edited 4 times in total.

Post #60 made 14 years ago
stux wrote:Another thought, did you end up spilling any mash water when you added your lid? That would've lost a few points there
Yes I spilled some, but it's hard to know exactly how much. My garage floor is now very sticky.

stux wrote:And did you perhaps measure your total mash volume? Might be able to work out a better grain wet displacement figure
I would say the total mash volume was 28.39 L. The exact volume of my 30 quart pot. Seriously, before putting the lid on I couldn't have fit an ounce more grain or water in the pot. It was to the rim. I didn't measure it again after the spill.
Last edited by de5m0mike on 14 Dec 2011, 10:29, edited 4 times in total.

Post #61 made 14 years ago
stux wrote: I think there is an issue in the chart... as it is getting confused by your -2% Kettle Loss... which I assume is due to measurement inaccuracies somewhere...
Amazing results ;)
You are correct. My measured end of boil volumes were incorrect. This one should be more accurate. I attribute the 1% loss to spillage.
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Last edited by de5m0mike on 14 Dec 2011, 10:36, edited 4 times in total.

Post #62 made 14 years ago
de5m0mike wrote:
stux wrote:Another thought, did you end up spilling any mash water when you added your lid? That would've lost a few points there
Yes I spilled some, but it's hard to know exactly how much. My garage floor is now very sticky.

stux wrote:And did you perhaps measure your total mash volume? Might be able to work out a better grain wet displacement figure
I would say the total mash volume was 28.39 L. The exact volume of my 30 quart pot. Seriously, before putting the lid on I couldn't have fit an ounce more grain or water in the pot. It was to the rim. I didn't measure it again after the spill.
Right

20.03L was the expected Strike at 20C, and the estimate was 20.39L at 70C (this is an iffy figure)

which leaves 8L for your wet grain

0.94L/KG displacement.

That looks pretty close to the dry grain displacement figure I use of 1.0L/KG

Basically, I find that when I add grain to strike water it displaces about 1.0L/KG (of the 20C) volume, but then the water seems to get absorbed into the grain, and it ends up displacing about 0.7L/KG total.

My previous maxi-biab calculator used to calculate a suggested reserve volume based on these differences... which means it probably would've suggested you reserve 3L before adding the grain, then add that back after you've gotten the grain good and wet.

Hmmm, I left that out of this calculator to simplify it ;)

0.94L sounds very high for an actual doughed in figure
Last edited by stux on 14 Dec 2011, 10:43, edited 4 times in total.
Fermenting: -
Cubed: -
Stirplate: -
On Tap: NS Summer Ale III (WY1272), Landlord III (WY1469), Fighter's 70/- II (WY1272), Roast Porter (WY1028), Cider, Soda
Next: Munich Helles III

5/7/12

Post #63 made 14 years ago
Still, you beat the End of Boil Efficiency (78.8 vs 78%) :)
wee heavy chart.png
Nice results.

I suspect your First Runnings might've had a higher gravity than you measured ;). You stirred thoroughly before taking the reading?


<50% efficiency without the sparge ;)
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Last edited by stux on 14 Dec 2011, 10:50, edited 4 times in total.
Fermenting: -
Cubed: -
Stirplate: -
On Tap: NS Summer Ale III (WY1272), Landlord III (WY1469), Fighter's 70/- II (WY1272), Roast Porter (WY1028), Cider, Soda
Next: Munich Helles III

5/7/12

Post #64 made 14 years ago
stux wrote:Still, you beat the End of Boil Efficiency (78.8 vs 78%) :)

Nice results.

I suspect your First Runnings might've had a higher gravity than you measured ;). You stirred thoroughly before taking the reading?


<50% efficiency without the sparge ;)

I honestly can't say how well it was stirred. I had a couple friends over to help with this and I put one of them in charge of the refractometer. I double checked the reading but didn't watch him collect the sample.
Last edited by de5m0mike on 14 Dec 2011, 21:01, edited 4 times in total.

Post #65 made 14 years ago
stux wrote: Basically, I find that when I add grain to strike water it displaces about 1.0L/KG (of the 20C) volume, but then the water seems to get absorbed into the grain, and it ends up displacing about 0.7L/KG total.
I could see that. When I first started adding the grain there were a couple times where the thick mash was actually rounded up over the top of the pot, but as I carefully stirred it in it eventually came down pretty even with the top of the pot.
Last edited by de5m0mike on 14 Dec 2011, 21:32, edited 4 times in total.

Post #67 made 13 years ago
Very good thread! I am considering a big beer 1.090 or so for my next batch and have been spending much brain power on how to achieve this with my equipment. This thread has been very helpful with my thought process. I am considering a slightly different technique and have a 10 gallon kettle. But thank you for this thread! :clap: :salute:

Post #68 made 13 years ago
I transfered this to secondary yesterday. Gravity had dropped to 1.031. ABV so far is 9.6%. I was hopping to hit the 10% mark though. We'll see if more time get's me there or If I'll need to get creative.
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